本书内容分为两部分。第一部分介绍化工原理实验涉及的理论知识，涵盖了科学安排实验和定量评价实验结果的方法，以及传统和现代的实验方法、测试技术与技巧，具体包括实验误差的分析与估算、实验数据处理、正交试验设计方法和化工实验参数测量技术；第二部分主要介绍化工单元操作实验，包括流体流动综合实验、传热综合实验、正交过滤实验、多相搅拌实验、洞道干燥实验、精馏实验、吸收实验和萃取实验，每个实验包含了实验目的、实验原理、操作步骤、注意事项、实验流程图和实验报告要求等，同时还介绍了化工实验室安全规定和相关的安全知识。
本书注重化工基础实验中的共性问题，拓宽基础，有较强的通用性，既可作为高等学校化工、化学、环境工程、食品科学与工程、材料等专业的国际化教材，又可供科研和实验工作者参考。
- 前辅文
- Introduction
- Chapter 1 Estimation and Analysis of Experimental Errors
- 1.1 Experimental Errors
- 1.1.1 Direct and Indirect Errors
- 1.1.2 True Value of Experimental Data
- 1.1.3 Definition and Representation of Error
- 1.1.4 Classification of Errors
- 1.1.5 Precision, Trueness and Accuracy
- 1.2 Significant Digit and Notation of Experimental Data
- 1.2.1 Significant Digit
- 1.2.2 Rounding Off Rules
- 1.2.3 Significant Digit of Direct Measurement Value
- 1.2.4 Significant Digit of Indirect Measurement Value
- 1.3 Error Estimation for Direct Measurement Value
- 1.3.1 Error Estimation for Once Measurement Value
- 1.3.2 Error Estimation for Multiple Measurements
- 1.4 Error Estimation of Indirect Measurement Value
- 1.4.1 General Function of Error Transfer
- 1.4.2 Application of Error Transfer Function
- 1.4.3 Application of Error Analysis
- List of Symbols
- Exercises
- Chapter 2 Experimental Data Processing
- 2.1 Tabular Method and Graphical Method
- 2.1.1 Tabular Method
- 2.1.2 Graphical Method
- 2.2 Experimental Data Regression Analysis
- 2.2.1 Definition and Content of Regression Analysis
- 2.2.2 Regression Expression Selection
- 2.2.3 Simple Linear Regression
- 2.2.4 Multivariable Linear Regression
- 2.2.5 Nonlinear Regression
- List of Symbols
- Exercises
- Chapter 3 Orthogonal Experimental Design Method
- 3.1 The Advantages of Orthogonal Experimental Design Method
- 3.2 Orthogonal Array and Its Characteristics
- 3.2.1 Equal Level Orthogonal Array
- 3.2.2 Mixed Level Orthogonal Array
- 3.3 The Interaction between Experimental Factors
- 3.3.1 The Definition of Interaction
- 3.3.2 The Discrimination of Interaction
- 3.4 Orthogonal Array Header Design
- 3.4.1 The Header Design with Interaction Effect
- 3.4.2 Header Design without Interaction Effect
- 3.5 The Basic Principles of Choosing an Orthogonal Array
- 3.6 The Operating Method of An Orthogonal Experiment
- 3.7 The Range Analysis of the Orthogonal Experimental Results
- 3.8 The Variance Analysis of the Orthogonal Experimental Results
- List of Symbols
- Exercises
- Chapter 4 Measurement of Common Physical Parameters in Chemical Industry
- 4.1 Basic Technical Performance of Measuring Instruments
- 4.1.1 Characteristics of Measuring Instrument
- 4.1.2 Measuring Instrument Selection Principle
- 4.2 Pressure Difference Measurement
- 4.2.1 Pressure Gauge and Differential Pressure Gauge
- 4.2.2 Pressure Difference Transducer
- 4.2.3 The Calibration of Pressure Gauge
- 4.2.4 Some Technological Matters in the Use of Pressure Gauge
- 4.3 Flow Measurement Techniques
- 4.3.1 Throttling Flowmeter
- 4.3.2 Rotameter
- 4.3.3 Turbine Flowmeter
- 4.3.4 Test and Calibration of Flowmeter
- 4.4 Temperature Measurement Techniques
- 4.4.1 Thermocouple
- 4.4.2 Resistance Temperature Detector (RTD)
- 4.4.3 Using Techniques in the Thermometer
- 4.4.4 The Calibration of Thermometer
- List of Symbols
- Exercises
- Appendix
- Appendix 1 Table of Correlation Coefficient
- Appendix 2 F Value Table
- Appendix 3 Common Orthogonal Array
- Laboratory Safety Rules
- Experiment 1 Experiment of Fluid Dynamics
- Experiment 1a Determination of Fluid Resistance
- Experiment 1b Performance Measurement of Centrifugal Pump
- Experiment 1c Determination of Flowmeter Performance
- Experiment 2 Heat Transfer Experiment
- Experiment 3 Application of Orthogonal Method in the Filtration Experiment
- Experiment 4 Multi-phase Agitation
- Experiment 5 Distillation
- Experiment 6 Packed Absorption Experiment
- Experiment 7 Extraction Experiment
- Experiment 8 Measurement of Drying Rate Curve
- Appendix Laboratory Safety Information
