本书根据中国药科大学“双一流”建设和化学基础课程教学改革的需要编写,采用中英双语对照形式,注重对学生化学实验基本知识、实验操作技能的掌握,以及实验研究方法的启蒙与初步训练。
全书分为“基本要求与实验室规则”“实验基本操作与技能”“实验数据的处理”“实验部分”和附录。实验部分结合了药学相关内容,包括无机制备、无机定性分析、化学定量分析、化学常数测定,既可独立开设,也可以对其中的一些实验稍加整合,作为系列实验进行。附录部分除了常用数据表,还有药典中常见的无机离子鉴别。
本书可作为高等学校药学类专业本科生的基础化学实验课程教材,也可供医学、食品及化学化工等专业学生和社会学习者参考。
- 前辅文
- Part 1 Laboratory General Information
- 1.1 Learning Objectives of the Course
- 1.2 General Guidelines
- 1.3 Honor Principle
- 1.4 General Safety Rules
- Part 2 General Equipment and Lab Techniques
- 2.1 General Equipment
- 2.2 Cleaning Laboratory Glassware
- 2.3 Digital Balance and Weighing
- 2.4 Separation of Solids from Liquids
- 2.5 Heating
- 2.6 Measuring and Delivering Liquid
- 2.7 pH Meter and pH Measurement
- 2.8 Notebooks
- 2.9 Analysis of Data and Presentation of Results
- Part 3 Quantitative Treatment of Data
- 3.1 Precision of Instrument Readings and Other Raw Data
- 3.2 Absolute and Relative Uncertainty
- 3.3 Accuracy and Precision
- 3.4 Error
- 3.5 Average Deviation and Standard Deviation
- 3.6 Significant Figure
- 3.7 Statistics Applied to Small Data Sets
- 3.8 Propagation of Indeterminate Errors
- Part 4 Experiments
- Experiment 1 Checking and Cleaning Equipment
- Experiment 2 Weighing Exercise and Preparing Solutions
- Experiment 3 Determination of the Water of Crystallization in Barium Chloride
- Experiment 4 Preparation of Ferrous Ammonium Sulfate Hexahydrate
- Experiment 5 Preparation of Zinc Gluconate
- Experiment 6 Preparation of Medicinal Sodium Chloride and Examination of Impurities Limitation
- Experiment 7 Synthesis of Potassium Aluminum Sulfate (Alum)
- Experiment 8 Qualitative Analysis of Cations (1)
- Experiment 9 Qualitative Analysis of Cations (2)
- Experiment 10 Designing Scheme for Qualitative Analysis of Cations
- Experiment 11 Calibration of Volumetric Glassware
- Experiment 12 Preparation and Standardization of a Standard Sodium Hydroxide Solution
- Experiment 13 Preparation and Standardization of a Standard solution of Hydrochloric Acid
- Experiment 14 Determination of Aspirin (acetylsalicylic acid) using Back Titration
- Experiment 15 Determination of Medicinal Zinc Oxide
- Experiment 16 Determination of Borax for Pharmaceutical Use
- Experiment 17 Determination of a Mixed Base
- Experiment 18 Preparation and Standardization of EDTA Solution
- Experiment 19 Content Assay of Zinc In Medicinal Zinc Gluconate
- Experiment 20 Determination of Water Hardness
- Experiment 21 Determination of Aluminium Potassium Sulfate in Alum
- Experiment 22 Precipitation Titration: Determination of Chloride by Mohr Method
- Experiment 23 Preparation and Standardization of Perchloric Acid in Non-aqueous Solvent
- Experiment 24 Determination of Sodium Salicylate in Non-aqueous Solvent
- Experiment 25 Preparation and Standardization of Potassium Permanganate Solution
- Experiment 26 Assay of Ferrous Ammonium Sulfate
- Experiment 27 Determination of Medical Hydrogen Peroxide
- Experiment 28 Preparation and Standardization of 0.05 molL−1 Iodine Solution
- Experiment 29 Iodimetric Titration of Ascorbic Acid in Vitamin C Tablets
- Experiment 30 Determination of Dissociation Constant of Weak Acid
- Experiment 31 Buffer Action and Buffer Solution
- Experiment 32 Determining Coordination Number of [Ag(NH3)n]+ Complex
- Experiment 33 Determination of Reaction Rate and Activation Energy
- Experiment 34 Determination of Ksp of Silver Acetate
- Part 5 Appendix
- 5.1 Identification Tests of Common Inorganic Ions
- 5.2 Ionization Constants of Inorganic Acids and Bases
- 5.3 Common Primary Standards
- 5.4 Common pH Buffer Solution
- 5.5 Common Indicator